Table 1.  Crystal data and structure refinement for miah_16june13_0ma.
Identification code 	shelx
Empirical formula 	C73 H34 B2 Cl2 F40 Ir2 N4 O2
Formula weight 	2235.96
Temperature 	100(2) K
Wavelength 	0.71073 Å
Crystal system 	Orthorhombic
Space group 	P b a 2
Unit cell dimensions	a = 16.454(4) Å	a= 90°.
	b = 22.905(5) Å	b= 90°.
	c = 9.7212(19) Å	g = 90°.
Volume	3663.8(14) Å3
Z	2
Density (calculated)	2.027 Mg/m3
Absorption coefficient	3.856 mm-1
F(000)	2148
Crystal size	0.320 x 0.170 x 0.050 mm3
Theta range for data collection	2.095 to 28.468°.
Index ranges	-21<=h<=21, -30<=k<=30, -12<=l<=12
Reflections collected	34924
Independent reflections	9125 [R(int) = 0.0186]
Completeness to theta = 25.000°	99.9 % 
Refinement method	Full-matrix least-squares on F2
Data / restraints / parameters	9125 / 22 / 594
Goodness-of-fit on F2	1.035
Final R indices [I>2sigma(I)]	R1 = 0.0141, wR2 = 0.0323
R indices (all data)	R1 = 0.0157, wR2 = 0.0329
Absolute structure parameter	-0.0031(14)
Extinction coefficient	n/a
Largest diff. peak and hole	0.519 and -0.467 e.Å-3

Table 2.  Atomic coordinates ( x 104) and equivalent isotropic displacement parameters (Å2x 103)
for miah_16june13_0ma.  U(eq) is defined as one third of the trace of the orthogonalized Uij tensor.
________________________________________________________________________________
	x	y	z	U(eq)
________________________________________________________________________________
C(1)	3030(2)	689(1)	6987(3)	19(1)
C(2)	3901(2)	222(1)	5577(3)	27(1)
C(3)	3660(2)	-162(1)	6532(3)	27(1)
C(4)	2738(2)	-160(2)	8554(4)	32(1)
C(5)	3599(2)	1247(1)	4958(4)	31(1)
C(6)	1310(2)	1225(2)	6237(4)	34(1)
C(7)	1687(2)	1777(2)	6113(4)	38(1)
C(8)	1528(3)	2080(2)	7347(5)	48(1)
C(9)	1090(3)	1722(3)	8193(4)	54(1)
C(10)	946(2)	1188(2)	7527(5)	50(1)
C(11)	2542(3)	1099(3)	9602(4)	29(1)
O(1)	2684(2)	997(2)	10731(4)	48(1)
C(12)	3350(3)	1855(4)	7972(9)	34(1)
C(11B)	3180(30)	1790(30)	8130(70)	34(1)
O(1B)	3837(16)	1981(10)	8197(18)	48(1)
C(12B)	2560(30)	1027(19)	10010(50)	29(1)
C(13)	2693(2)	3070(1)	1878(3)	15(1)
C(14)	3052(2)	2542(1)	2198(3)	18(1)
C(15)	3776(2)	2349(1)	1638(3)	20(1)
C(16)	4179(2)	2687(1)	700(3)	21(1)
C(17)	3868(2)	3227(1)	371(3)	20(1)
C(18)	3150(2)	3404(1)	966(3)	17(1)
C(19)	1258(2)	2833(1)	3244(3)	18(1)
C(20)	805(2)	2882(1)	4438(3)	24(1)
C(21)	223(2)	2479(2)	4841(4)	32(1)
C(22)	85(2)	1993(2)	4054(4)	33(1)
C(23)	523(2)	1919(1)	2870(5)	27(1)
C(24)	1081(2)	2337(1)	2486(3)	21(1)
C(25)	2269(2)	3793(1)	3715(3)	18(1)
C(26)	2649(2)	3580(2)	4890(3)	23(1)
C(27)	3124(2)	3917(2)	5762(4)	31(1)
C(28)	3250(2)	4494(2)	5457(4)	31(1)
C(29)	2883(2)	4729(2)	4316(4)	28(1)
C(30)	2401(2)	4383(1)	3487(3)	21(1)
C(31)	1232(2)	3658(1)	1513(3)	15(1)
C(32)	1177(2)	3555(1)	109(3)	19(1)
C(33)	576(2)	3781(1)	-724(3)	22(1)
C(34)	-15(2)	4134(1)	-170(3)	24(1)
C(35)	-6(2)	4240(1)	1222(3)	19(1)
C(36)	605(2)	4008(1)	2009(3)	17(1)
N(1)	3517(2)	742(1)	5866(3)	21(1)
N(2)	3126(2)	125(1)	7388(2)	23(1)
B(1)	1862(2)	3339(1)	2598(3)	16(1)
Ir(1)	2306(1)	1318(1)	7822(1)	19(1)
F(1)	2706(1)	2171(1)	3112(2)	22(1)
F(2)	4083(1)	1826(1)	2001(2)	28(1)
F(3)	4873(1)	2499(1)	129(2)	27(1)
F(4)	4266(1)	3572(1)	-513(2)	28(1)
F(5)	2892(1)	3942(1)	618(2)	22(1)
F(6)	922(1)	3336(1)	5305(2)	30(1)
F(7)	-185(1)	2558(1)	6028(3)	44(1)
F(8)	-466(1)	1593(1)	4437(3)	48(1)
F(9)	399(1)	1444(1)	2075(2)	38(1)
F(10)	1452(1)	2243(1)	1265(2)	24(1)
F(11)	2593(1)	3009(1)	5204(2)	30(1)
F(12)	3469(2)	3676(1)	6870(2)	43(1)
F(13)	3722(1)	4825(1)	6269(2)	45(1)
F(14)	2983(1)	5300(1)	4015(2)	36(1)
F(15)	2061(1)	4661(1)	2412(2)	24(1)
F(16)	1724(1)	3212(1)	-539(2)	24(1)
F(17)	564(1)	3658(1)	-2077(3)	31(1)
F(18)	-600(1)	4362(1)	-967(2)	34(1)
F(19)	-597(1)	4563(1)	1795(2)	27(1)
F(20)	568(1)	4133(1)	3368(2)	20(1)
Cl(2B)	4170(20)	5088(16)	800(30)	121(2)
C(37B)	5180(20)	5130(40)	1598(17)	57(3)
Cl(1)	5000	5000	3441(3)	80(1)
Cl(2)	4831(5)	4962(5)	404(5)	121(2)
C(37)	5552(7)	5104(5)	1813(6)	57(3)
________________________________________________________________________________
Table 3.   Bond lengths [Å] and angles [°] for miah_16june13_0ma.
_____________________________________________________
C(1)-N(2) 	1.358(4)
C(1)-N(1) 	1.358(4)
C(1)-Ir(1) 	2.036(3)
C(2)-C(3) 	1.340(5)
C(2)-N(1) 	1.376(4)
C(2)-H(2) 	0.9500
C(3)-N(2) 	1.378(4)
C(3)-H(3) 	0.9500
C(4)-N(2) 	1.456(4)
C(4)-H(4A) 	0.9800
C(4)-H(4B) 	0.9800
C(4)-H(4C) 	0.9800
C(5)-N(1) 	1.462(4)
C(5)-H(5A) 	0.9800
C(5)-H(5B) 	0.9800
C(5)-H(5C) 	0.9800
C(6)-C(10) 	1.392(6)
C(6)-C(7) 	1.413(6)
C(6)-Ir(1) 	2.260(3)
C(6)-H(6) 	0.9500
C(7)-C(8) 	1.411(6)
C(7)-Ir(1) 	2.215(3)
C(7)-H(7) 	0.9500
C(8)-C(9) 	1.366(7)
C(8)-Ir(1) 	2.214(4)
C(8)-H(8) 	0.9500
C(9)-C(10) 	1.404(7)
C(9)-Ir(1) 	2.234(4)
C(9)-H(9) 	0.9500
C(10)-Ir(1) 	2.276(4)
C(10)-H(10) 	0.9500
C(11)-O(1) 	1.146(6)
C(11)-Ir(1) 	1.843(4)
C(12)-Ir(1) 	2.118(4)
C(12)-H(12A) 	0.9800
C(12)-H(12B) 	0.9800
C(12)-H(12C) 	0.9800
C(11B)-O(1B) 	1.16(3)
C(11B)-Ir(1) 	1.83(4)
C(12B)-Ir(1) 	2.27(4)
C(12B)-H(12D) 	0.9800
C(12B)-H(12E) 	0.9800
C(12B)-H(12F) 	0.9800
C(13)-C(14) 	1.381(4)
C(13)-C(18) 	1.391(4)
C(13)-B(1) 	1.655(4)
C(14)-F(1) 	1.355(3)
C(14)-C(15) 	1.383(4)
C(15)-F(2) 	1.348(3)
C(15)-C(16) 	1.368(4)
C(16)-F(3) 	1.341(3)
C(16)-C(17) 	1.376(4)
C(17)-F(4) 	1.339(3)
C(17)-C(18) 	1.376(4)
C(18)-F(5) 	1.347(3)
C(19)-C(24) 	1.384(4)
C(19)-C(20) 	1.384(4)
C(19)-B(1) 	1.651(4)
C(20)-F(6) 	1.353(4)
C(20)-C(21) 	1.386(5)
C(21)-F(7) 	1.347(4)
C(21)-C(22) 	1.370(6)
C(22)-F(8) 	1.341(4)
C(22)-C(23) 	1.368(6)
C(23)-F(9) 	1.350(4)
C(23)-C(24) 	1.380(4)
C(24)-F(10) 	1.352(3)
C(25)-C(30) 	1.387(4)
C(25)-C(26) 	1.390(4)
C(25)-B(1) 	1.646(4)
C(26)-F(11) 	1.347(4)
C(26)-C(27) 	1.387(5)
C(27)-F(12) 	1.337(4)
C(27)-C(28) 	1.370(5)
C(28)-F(13) 	1.342(4)
C(28)-C(29) 	1.374(5)
C(29)-F(14) 	1.348(4)
C(29)-C(30) 	1.381(4)
C(30)-F(15) 	1.345(4)
C(31)-C(32) 	1.388(4)
C(31)-C(36) 	1.391(4)
C(31)-B(1) 	1.650(4)
C(32)-F(16) 	1.350(4)
C(32)-C(33) 	1.379(4)
C(33)-F(17) 	1.345(4)
C(33)-C(34) 	1.376(5)
C(34)-F(18) 	1.342(3)
C(34)-C(35) 	1.375(4)
C(35)-F(19) 	1.342(3)
C(35)-C(36) 	1.371(4)
C(36)-F(20) 	1.354(3)
Cl(2B)-C(37B)#1 	1.41(7)
Cl(2B)-C(37B) 	1.843(10)
C(37B)-C(37B)#1 	0.85(11)
C(37B)-Cl(2B)#1 	1.41(7)
C(37B)-Cl(1) 	1.841(10)
C(37B)-H(37C) 	0.9700
C(37B)-H(37D) 	0.9700
Cl(1)-C(37) 	1.841(8)
Cl(1)-C(37)#1 	1.841(8)
Cl(1)-C(37B)#1 	1.841(10)
Cl(2)-Cl(2)#1 	0.583(16)
Cl(2)-C(37)#1 	1.515(9)
Cl(2)-C(37) 	1.841(8)
C(37)-Cl(2)#1 	1.515(9)
C(37)-C(37)#1 	1.88(2)
C(37)-H(37A) 	0.9700
C(37)-H(37B) 	0.9700

N(2)-C(1)-N(1)	104.2(2)
N(2)-C(1)-Ir(1)	128.7(2)
N(1)-C(1)-Ir(1)	127.0(2)
C(3)-C(2)-N(1)	106.9(3)
C(3)-C(2)-H(2)	126.5
N(1)-C(2)-H(2)	126.5
C(2)-C(3)-N(2)	107.0(3)
C(2)-C(3)-H(3)	126.5
N(2)-C(3)-H(3)	126.5
N(2)-C(4)-H(4A)	109.5
N(2)-C(4)-H(4B)	109.5
H(4A)-C(4)-H(4B)	109.5
N(2)-C(4)-H(4C)	109.5
H(4A)-C(4)-H(4C)	109.5
H(4B)-C(4)-H(4C)	109.5
N(1)-C(5)-H(5A)	109.5
N(1)-C(5)-H(5B)	109.5
H(5A)-C(5)-H(5B)	109.5
N(1)-C(5)-H(5C)	109.5
H(5A)-C(5)-H(5C)	109.5
H(5B)-C(5)-H(5C)	109.5
C(10)-C(6)-C(7)	108.6(3)
C(10)-C(6)-Ir(1)	72.8(2)
C(7)-C(6)-Ir(1)	69.9(2)
C(10)-C(6)-H(6)	125.7
C(7)-C(6)-H(6)	125.7
Ir(1)-C(6)-H(6)	123.3
C(8)-C(7)-C(6)	106.7(4)
C(8)-C(7)-Ir(1)	71.4(2)
C(6)-C(7)-Ir(1)	73.3(2)
C(8)-C(7)-H(7)	126.7
C(6)-C(7)-H(7)	126.7
Ir(1)-C(7)-H(7)	120.5
C(9)-C(8)-C(7)	108.3(4)
C(9)-C(8)-Ir(1)	72.9(2)
C(7)-C(8)-Ir(1)	71.5(2)
C(9)-C(8)-H(8)	125.9
C(7)-C(8)-H(8)	125.9
Ir(1)-C(8)-H(8)	121.4
C(8)-C(9)-C(10)	109.5(3)
C(8)-C(9)-Ir(1)	71.3(2)
C(10)-C(9)-Ir(1)	73.5(2)
C(8)-C(9)-H(9)	125.2
C(10)-C(9)-H(9)	125.2
Ir(1)-C(9)-H(9)	121.6
C(6)-C(10)-C(9)	106.9(4)
C(6)-C(10)-Ir(1)	71.5(2)
C(9)-C(10)-Ir(1)	70.3(2)
C(6)-C(10)-H(10)	126.6
C(9)-C(10)-H(10)	126.6
Ir(1)-C(10)-H(10)	123.4
O(1)-C(11)-Ir(1)	176.0(5)
Ir(1)-C(12)-H(12A)	109.5
Ir(1)-C(12)-H(12B)	109.5
H(12A)-C(12)-H(12B)	109.5
Ir(1)-C(12)-H(12C)	109.5
H(12A)-C(12)-H(12C)	109.5
H(12B)-C(12)-H(12C)	109.5
O(1B)-C(11B)-Ir(1)	164(6)
Ir(1)-C(12B)-H(12D)	109.5
Ir(1)-C(12B)-H(12E)	109.5
H(12D)-C(12B)-H(12E)	109.5
Ir(1)-C(12B)-H(12F)	109.5
H(12D)-C(12B)-H(12F)	109.5
H(12E)-C(12B)-H(12F)	109.5
C(14)-C(13)-C(18)	113.2(3)
C(14)-C(13)-B(1)	125.7(2)
C(18)-C(13)-B(1)	120.8(2)
F(1)-C(14)-C(13)	121.2(2)
F(1)-C(14)-C(15)	114.8(2)
C(13)-C(14)-C(15)	124.0(3)
F(2)-C(15)-C(16)	119.8(3)
F(2)-C(15)-C(14)	120.3(3)
C(16)-C(15)-C(14)	120.0(3)
F(3)-C(16)-C(15)	120.4(3)
F(3)-C(16)-C(17)	120.7(3)
C(15)-C(16)-C(17)	118.9(3)
F(4)-C(17)-C(16)	119.8(3)
F(4)-C(17)-C(18)	121.1(3)
C(16)-C(17)-C(18)	119.1(3)
F(5)-C(18)-C(17)	115.7(2)
F(5)-C(18)-C(13)	119.5(3)
C(17)-C(18)-C(13)	124.8(3)
C(24)-C(19)-C(20)	113.6(3)
C(24)-C(19)-B(1)	120.0(2)
C(20)-C(19)-B(1)	125.8(3)
F(6)-C(20)-C(19)	120.6(3)
F(6)-C(20)-C(21)	115.7(3)
C(19)-C(20)-C(21)	123.7(3)
F(7)-C(21)-C(22)	120.3(3)
F(7)-C(21)-C(20)	119.9(4)
C(22)-C(21)-C(20)	119.8(3)
F(8)-C(22)-C(23)	120.2(3)
F(8)-C(22)-C(21)	120.8(3)
C(23)-C(22)-C(21)	119.0(3)
F(9)-C(23)-C(22)	120.2(3)
F(9)-C(23)-C(24)	120.4(4)
C(22)-C(23)-C(24)	119.4(3)
F(10)-C(24)-C(23)	115.3(3)
F(10)-C(24)-C(19)	120.2(3)
C(23)-C(24)-C(19)	124.5(3)
C(30)-C(25)-C(26)	113.8(3)
C(30)-C(25)-B(1)	125.1(3)
C(26)-C(25)-B(1)	120.2(3)
F(11)-C(26)-C(27)	116.1(3)
F(11)-C(26)-C(25)	119.8(3)
C(27)-C(26)-C(25)	124.1(3)
F(12)-C(27)-C(28)	120.5(3)
F(12)-C(27)-C(26)	120.2(3)
C(28)-C(27)-C(26)	119.3(3)
F(13)-C(28)-C(27)	120.4(3)
F(13)-C(28)-C(29)	120.5(3)
C(27)-C(28)-C(29)	119.1(3)
F(14)-C(29)-C(28)	120.1(3)
F(14)-C(29)-C(30)	120.0(3)
C(28)-C(29)-C(30)	119.9(3)
F(15)-C(30)-C(29)	114.9(3)
F(15)-C(30)-C(25)	121.3(3)
C(29)-C(30)-C(25)	123.8(3)
C(32)-C(31)-C(36)	113.0(3)
C(32)-C(31)-B(1)	126.4(3)
C(36)-C(31)-B(1)	120.0(2)
F(16)-C(32)-C(33)	115.0(3)
F(16)-C(32)-C(31)	121.0(3)
C(33)-C(32)-C(31)	124.0(3)
F(17)-C(33)-C(34)	119.7(3)
F(17)-C(33)-C(32)	120.4(3)
C(34)-C(33)-C(32)	119.9(3)
F(18)-C(34)-C(35)	120.5(3)
F(18)-C(34)-C(33)	120.7(3)
C(35)-C(34)-C(33)	118.8(3)
F(19)-C(35)-C(36)	121.0(3)
F(19)-C(35)-C(34)	119.8(3)
C(36)-C(35)-C(34)	119.2(3)
F(20)-C(36)-C(35)	115.4(3)
F(20)-C(36)-C(31)	119.5(3)
C(35)-C(36)-C(31)	125.1(3)
C(1)-N(1)-C(2)	111.0(3)
C(1)-N(1)-C(5)	127.5(3)
C(2)-N(1)-C(5)	121.2(3)
C(1)-N(2)-C(3)	110.9(3)
C(1)-N(2)-C(4)	126.8(3)
C(3)-N(2)-C(4)	122.3(3)
C(25)-B(1)-C(31)	113.4(2)
C(25)-B(1)-C(19)	116.0(2)
C(31)-B(1)-C(19)	100.1(2)
C(25)-B(1)-C(13)	100.3(2)
C(31)-B(1)-C(13)	114.4(2)
C(19)-B(1)-C(13)	113.4(2)
C(11B)-Ir(1)-C(1)	91(2)
C(11)-Ir(1)-C(1)	93.40(19)
C(11)-Ir(1)-C(12)	85.6(3)
C(1)-Ir(1)-C(12)	88.0(3)
C(11B)-Ir(1)-C(8)	91(2)
C(11)-Ir(1)-C(8)	122.1(2)
C(1)-Ir(1)-C(8)	144.31(14)
C(12)-Ir(1)-C(8)	91.4(3)
C(11B)-Ir(1)-C(7)	101.6(18)
C(11)-Ir(1)-C(7)	158.5(2)
C(1)-Ir(1)-C(7)	107.78(13)
C(12)-Ir(1)-C(7)	98.5(2)
C(8)-Ir(1)-C(7)	37.15(15)
C(11B)-Ir(1)-C(9)	116(2)
C(11)-Ir(1)-C(9)	98.6(2)
C(1)-Ir(1)-C(9)	151.74(15)
C(12)-Ir(1)-C(9)	118.3(3)
C(8)-Ir(1)-C(9)	35.77(17)
C(7)-Ir(1)-C(9)	60.77(15)
C(11B)-Ir(1)-C(6)	137.5(19)
C(11)-Ir(1)-C(6)	140.1(2)
C(1)-Ir(1)-C(6)	94.92(11)
C(12)-Ir(1)-C(6)	133.6(2)
C(8)-Ir(1)-C(6)	60.82(13)
C(7)-Ir(1)-C(6)	36.79(14)
C(9)-Ir(1)-C(6)	59.95(13)
C(11B)-Ir(1)-C(12B)	83.0(19)
C(1)-Ir(1)-C(12B)	93.5(11)
C(8)-Ir(1)-C(12B)	122.2(11)
C(7)-Ir(1)-C(12B)	158.0(11)
C(9)-Ir(1)-C(12B)	97.7(11)
C(6)-Ir(1)-C(12B)	138.2(11)
C(11B)-Ir(1)-C(10)	151(2)
C(11)-Ir(1)-C(10)	106.9(2)
C(1)-Ir(1)-C(10)	115.62(14)
C(12)-Ir(1)-C(10)	151.8(3)
C(8)-Ir(1)-C(10)	60.50(17)
C(7)-Ir(1)-C(10)	60.94(16)
C(9)-Ir(1)-C(10)	36.26(17)
C(6)-Ir(1)-C(10)	35.73(15)
C(12B)-Ir(1)-C(10)	105.1(11)
C(37B)#1-Cl(2B)-C(37B)	26(5)
C(37B)#1-C(37B)-Cl(2B)#1	107(10)
C(37B)#1-C(37B)-Cl(1)	76.7(18)
Cl(2B)#1-C(37B)-Cl(1)	127(4)
C(37B)#1-C(37B)-Cl(2B)	47(6)
Cl(2B)#1-C(37B)-Cl(2B)	116(4)
Cl(1)-C(37B)-Cl(2B)	104.5(10)
C(37B)#1-C(37B)-H(37C)	153.5
Cl(2B)#1-C(37B)-H(37C)	91.4
Cl(1)-C(37B)-H(37C)	108.1
Cl(2B)-C(37B)-H(37C)	107.7
C(37B)#1-C(37B)-H(37D)	95.1
Cl(2B)#1-C(37B)-H(37D)	24.8
Cl(1)-C(37B)-H(37D)	103.4
Cl(2B)-C(37B)-H(37D)	123.6
H(37C)-C(37B)-H(37D)	108.7
C(37)-Cl(1)-C(37)#1	61.4(6)
C(37B)#1-Cl(1)-C(37B)	27(4)
Cl(2)#1-Cl(2)-C(37)#1	115.3(5)
Cl(2)#1-Cl(2)-C(37)	48.1(4)
C(37)#1-Cl(2)-C(37)	67.3(7)
Cl(2)#1-C(37)-Cl(1)	124.0(8)
Cl(2)#1-C(37)-Cl(2)	16.6(5)
Cl(1)-C(37)-Cl(2)	107.4(6)
Cl(2)#1-C(37)-C(37)#1	64.7(5)
Cl(1)-C(37)-C(37)#1	59.3(3)
Cl(2)-C(37)-C(37)#1	48.1(4)
Cl(2)#1-C(37)-H(37A)	100.8
Cl(1)-C(37)-H(37A)	109.4
Cl(2)-C(37)-H(37A)	110.2
C(37)#1-C(37)-H(37A)	124.3
Cl(2)#1-C(37)-H(37B)	105.3
Cl(1)-C(37)-H(37B)	108.2
Cl(2)-C(37)-H(37B)	113.4
C(37)#1-C(37)-H(37B)	127.4
H(37A)-C(37)-H(37B)	108.2
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Symmetry transformations used to generate equivalent atoms: 
#1 -x+1,-y+1,z 

Table 4.   Anisotropic displacement parameters (Å2x 103)for miah_16june13_0ma.  The anisotropic
displacement factor exponent takes the form: -2p2[ h2a*2U11 + ... + 2 h k a* b* U12 ]
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	U11	U22	U33	U23	U13	U12
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C(1)	15(1) 	23(1)	19(1) 	-1(1)	-3(1) 	2(1)
C(2)	20(2) 	30(2)	31(2) 	-6(1)	-1(1) 	9(1)
C(3)	24(2) 	26(2)	33(2) 	-3(1)	-6(1) 	8(1)
C(4)	38(2) 	29(2)	29(2) 	8(1)	-1(2) 	0(2)
C(5)	34(2) 	29(2)	30(2) 	5(1)	11(1) 	-1(1)
C(6)	34(2) 	35(2)	34(2) 	-16(1)	-16(2) 	20(2)
C(7)	32(2) 	46(2)	37(2) 	12(2)	-6(2) 	13(2)
C(8)	38(2) 	33(2)	71(3) 	-24(2)	-22(2) 	23(2)
C(9)	29(2) 	103(4)	31(2) 	-23(2)	-4(2) 	26(2)
C(10)	26(2) 	63(3)	59(4) 	9(2)	-4(2) 	-4(2)
C(11)	31(2) 	40(2)	15(3) 	0(2)	2(2) 	5(2)
O(1)	63(2) 	61(2)	21(2) 	1(2)	-5(2) 	14(2)
C(12)	24(3) 	42(3)	36(3) 	-11(2)	-4(3) 	-9(2)
C(11B)	24(3) 	42(3)	36(3) 	-11(2)	-4(3) 	-9(2)
O(1B)	63(2) 	61(2)	21(2) 	1(2)	-5(2) 	14(2)
C(12B)	31(2) 	40(2)	15(3) 	0(2)	2(2) 	5(2)
C(13)	14(1) 	16(1)	16(1) 	-3(1)	-2(1) 	0(1)
C(14)	16(1) 	18(1)	18(1) 	-1(1)	-1(1) 	1(1)
C(15)	16(1) 	16(1)	27(1) 	-4(1)	-3(1) 	4(1)
C(16)	11(1) 	28(2)	23(1) 	-7(1)	0(1) 	3(1)
C(17)	16(1) 	26(2)	17(1) 	0(1)	0(1) 	-3(1)
C(18)	18(1) 	15(1)	19(1) 	-1(1)	-1(1) 	0(1)
C(19)	15(1) 	18(1)	22(1) 	6(1)	-1(1) 	5(1)
C(20)	20(2) 	26(2)	24(1) 	8(1)	2(1) 	9(1)
C(21)	17(2) 	45(2)	33(2) 	18(2)	8(1) 	9(1)
C(22)	15(2) 	39(2)	44(2) 	22(2)	-1(1) 	-2(1)
C(23)	20(1) 	25(1)	37(2) 	6(2)	-9(2) 	-2(1)
C(24)	14(1) 	26(1)	24(2) 	5(1)	-3(1) 	3(1)
C(25)	15(1) 	23(1)	17(1) 	-5(1)	-2(1) 	6(1)
C(26)	23(2) 	28(2)	20(1) 	-4(1)	-4(1) 	10(1)
C(27)	25(2) 	45(2)	21(2) 	-12(1)	-9(1) 	15(2)
C(28)	20(2) 	38(2)	33(2) 	-20(1)	-7(1) 	5(1)
C(29)	20(2) 	27(2)	37(2) 	-14(1)	1(1) 	2(1)
C(30)	15(1) 	24(2)	23(2) 	-7(1)	-2(1) 	4(1)
C(31)	15(1) 	12(1)	18(1) 	1(1)	-2(1) 	-2(1)
C(32)	19(2) 	18(1)	20(1) 	1(1)	-1(1) 	-4(1)
C(33)	24(2) 	24(1)	19(1) 	4(1)	-7(1) 	-10(1)
C(34)	19(2) 	20(1)	32(2) 	10(1)	-12(1) 	-5(1)
C(35)	13(1) 	12(1)	33(2) 	4(1)	-2(1) 	-1(1)
C(36)	20(2) 	12(1)	20(1) 	1(1)	-2(1) 	-2(1)
N(1)	17(1) 	24(1)	23(1) 	-1(1)	0(1) 	2(1)
N(2)	23(1) 	21(1)	24(1) 	1(1)	-6(1) 	2(1)
B(1)	16(1) 	15(1)	17(2) 	-1(1)	-1(1) 	4(1)
Ir(1)	20(1) 	21(1)	15(1) 	-3(1)	-1(1) 	2(1)
F(1)	21(1) 	19(1)	26(1) 	7(1)	4(1) 	4(1)
F(2)	21(1) 	20(1)	42(1) 	-1(1)	2(1) 	9(1)
F(3)	15(1) 	34(1)	32(1) 	-6(1)	6(1) 	4(1)
F(4)	20(1) 	38(1)	27(1) 	7(1)	6(1) 	-3(1)
F(5)	21(1) 	19(1)	26(1) 	7(1)	1(1) 	2(1)
F(6)	35(1) 	33(1)	21(1) 	2(1)	9(1) 	13(1)
F(7)	31(1) 	62(2)	41(1) 	24(1)	21(1) 	13(1)
F(8)	26(1) 	49(1)	69(2) 	30(1)	3(1) 	-12(1)
F(9)	32(1) 	23(1)	60(1) 	5(1)	-14(1) 	-11(1)
F(10)	24(1) 	23(1)	27(1) 	-5(1)	1(1) 	-3(1)
F(11)	37(1) 	29(1)	24(1) 	2(1)	-9(1) 	11(1)
F(12)	44(1) 	59(1)	26(1) 	-10(1)	-20(1) 	19(1)
F(13)	35(1) 	50(1)	48(1) 	-29(1)	-18(1) 	4(1)
F(14)	30(1) 	26(1)	53(1) 	-16(1)	-7(1) 	-2(1)
F(15)	23(1) 	18(1)	31(1) 	0(1)	-5(1) 	-1(1)
F(16)	24(1) 	31(1)	18(1) 	-6(1)	0(1) 	1(1)
F(17)	35(1) 	42(1)	17(1) 	5(1)	-9(1) 	-12(1)
F(18)	27(1) 	36(1)	40(1) 	14(1)	-20(1) 	-2(1)
F(19)	15(1) 	20(1)	45(1) 	3(1)	-3(1) 	4(1)
F(20)	18(1) 	21(1)	22(1) 	-3(1)	1(1) 	5(1)
Cl(2B)	126(5) 	114(3)	124(3) 	-29(3)	-25(3) 	-8(4)
C(37B)	40(6) 	49(6)	82(8) 	-4(5)	-18(6) 	-11(6)
Cl(1)	53(1) 	71(1)	118(2) 	0	0 	0(1)
Cl(2)	126(5) 	114(3)	124(3) 	-29(3)	-25(3) 	-8(4)
C(37)	40(6) 	49(6)	82(8) 	-4(5)	-18(6) 	-11(6)
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Table 5.   Hydrogen coordinates ( x 104) and isotropic displacement parameters (Å2x 103)
for miah_16june13_0ma.
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	x 	y 	z 	U(eq)
________________________________________________________________________________

H(2)	4267	150	4841	32
H(3)	3826	-558	6606	33
H(4A)	3071	-104	9379	48
H(4B)	2683	-579	8365	48
H(4C)	2198	10	8703	48
H(5A)	3340	1162	4072	47
H(5B)	4176	1331	4813	47
H(5C)	3335	1586	5381	47
H(6)	1306	928	5555	41
H(7)	1988	1916	5347	46
H(8)	1698	2467	7555	57
H(9)	911	1820	9093	65
H(10)	656	864	7887	60
H(12A)	3372	2032	8889	51
H(12B)	3322	2163	7274	51
H(12C)	3838	1619	7822	51
H(12D)	3023	759	10021	43
H(12E)	2079	828	10383	43
H(12F)	2683	1369	10582	43
H(37C)	5378	5528	1492	68
H(37D)	5623	4864	1381	68
H(37A)	5751	5502	1761	68
H(37B)	6017	4843	1810	68
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